Lts of Raman (52-289), PS b36((Si2O7)six(Si4Figure 11.(44-271), Pb33(Si2O7)6(Si4O13)3 (44-273), P 692), PCS–Pb8Ca(Si2O7)3 (32-514), CS–Ca2SiO4 (23-1042), Qz–quartz SiO2 (33-1161), Ca3(PO4)2 (9-348), Ph. am. morphous phase.three.three. The Black Bead from Opening No. 3A Both sides of the bead (the leading and bottom) had been examined. Representative SEM-EDS evaluation results are shown in Figure 10 and benefits of Raman microspectroscopy analysis, in Figure 11.Figure 10. Backscattered electron (BSE) the surface of surface in the black (2-Hydroxypropyl)-β-cyclodextrin References chemical analyses obtained at Figure 10. Backscattered electron (BSE) image ofimage of thethe black bead (a,b). For bead (a,b). For chemical the analyses obtained at Table four. points numbered 1, see the points numbered 1, see Table 4. Table 4. Chemical composition, in weight percentage, of your black bead. For all elements (except anion Cl), the composition is expressed as oxides weight . The precise positions on the analysed points are shown in Figure ten.CO1 b.d.l.2 12.Analysed Points three four ten.40 b.d.l.five b.d.l.6 b.d.l.Minerals 2021, 11,13 ofTable four. Chemical composition, in weight percentage, in the black bead. For all Cyclosporin H Biological Activity components (exceptMinerals 2021, 11, x FOR PEER Assessment Cl), the composition is expressed as oxides weight . The exact positions of your analysed 13 of 25 anionpoints are shown in Figure ten.b.d.l.–below detection limit.N2O5 Na2O CO2 MgO N2 O2O3 Al5 Na2 O SiO MgO 2 P2 three Al2 OO5 SiO2 three SO P2PbO2 O5 SO3 Cl PbO2 K2O Cl K2 O CaO CaO MnO MnO Fe2O3 Fe2 O3 CoO CoO NiO NiO CuO CuO ZnO ZnO Total Totalb.d.l. 1 12.25 b.d.l. 3.39 b.d.l. 3.02 12.25 63.20 three.39 0.58 3.02 63.20 0.41 0.58 two.09 0.41 0.81 two.09 2.32 0.81 2.32 6.09 6.09 3.85 3.85 1.13 1.13 0.20 0.20 0.15 0.15 0.31 0.31 0.20 0.20 100.00 one hundred.b.d.l. 22.70 12.40 1.02 b.d.l. 2.94 two.70 38.35 1.02 7.22 2.94 38.35 0.42 7.22 18.14 0.42 two.18 18.14 1.14 2.18 1.14 9.46 9.46 1.14 1.14 1.87 1.87 b.d.l. b.d.l. 0.28 0.28 0.40 0.40 0.32 0.32 one hundred.00 100.Analysed Pointsb.d.l.b.d.l.b.d.l.5 10.48 b.d.l. 3.11 b.d.l. 3.35 ten.48 61.59 three.11 0.63 3.35 61.59 0.47 0.63 2.38 0.47 1.05 2.38 two.20 1.05 two.20 7.87 7.87 five.15 5.15 1.72 1.72 b.d.l. b.d.l. b.d.l. b.d.l. b.d.l. b.d.l. b.d.l. b.d.l. 100.3 3.46 ten.40 1.01 b.d.l. two.88 three.46 46.03 1.01 6.23 2.88 46.03 0.35 6.23 14.83 0.35 2.34 14.83 1.12 2.34 1.12 7.69 7.69 1.03 1.03 1.57 1.57 0.18 0.18 0.27 0.27 0.36 0.36 0.27 0.27 one hundred.four 4.48 b.d.l. 1.13 b.d.l. 4.ten four.48 77.57 1.13 0.44 4.10 77.57 0.42 0.44 0.83 0.42 1.45 0.83 1.69 1.45 1.69 3.68 three.68 1.10 1.ten two.ten 2.ten 0.11 0.11 0.22 0.22 0.27 0.27 0.41 0.41 100.100.one hundred.100.b.d.l. 6 11.09 b.d.l. 3.36 b.d.l. 2.85 11.09 62.47 three.36 0.81 two.85 62.47 0.46 0.81 2.01 0.46 0.81 two.01 three.66 0.81 3.66 five.74 5.74 three.84 3.84 1.48 1.48 0.34 0.34 0.17 0.17 0.35 0.35 0.55 0.55 100.00 100.b.d.l.–below detection limit.Figure 11. Representative characteristic Raman spectra of the surface of your black bead. Figure 11. Representative characteristic Raman spectra from the surface from the black bead.EDS chemical evaluation of bead surface (Figure 10, Table four, points 1, five and six) and six) EDS chemical analysis of thethe bead surface (Figure 10, Table four, points 1, 5mainly primarily the presence of Si (imply SiO2 : 66.21 6.56 six.56 wt), Na Na2 O: 9.58 3.01 showed showed the presence of Si (imply SiO2: 66.21 wt), Na (mean (imply Na2O: 9.58 three.01 Ca (mean CaO: CaO: 1.49 wt), K (imply K2 O: 2.47 0.73 0.73 wt), Mg (mean wt),wt), Ca (mean 5.85 5.85 1.49 wt), K (mean K2O: 2.47 wt), Mg (mean MgO: MgO: two.75 0.94 wt) and Al Al2 O Al2O 3.33 0.48 wt). Also, the.
